Alpha particle X-ray spectrometer

An alpha particle X-ray spectrometer (APXS) is a spectrometer that analyses the chemical element composition of a sample from the scattered alpha particles, and fluorescent X-rays after the sample is irradiated with alpha particles and X-rays from radioactive sources.[1] This method of analysing the elemental composition of a sample is most often used on space missions, which require low weight, small size, and minimal power consumption. Other methods (e.g. mass spectrometry) are faster, and do not require the use of radioactive materials, but require larger equipment with less modest power requirements. A variation is the alpha proton X-ray spectrometer, such as on the Pathfinder mission, which also detects protons.

APXS is also an abbreviation for APache eXtenSion tool, an extension for Apache web servers.
Alpha particle X-ray spectrometer (top left), APXS at the back of the Mars Pathfinder Sojourner rover (right), MSL Curiosity's alpha particle X-ray spectrometer, with a ruler (bottom left).

Over the years several modified versions of this type of instrument such as APS (without X-ray spectrometer) or APXS have been flown: Surveyor 5-7,[2] Mars Pathfinder,[3] Mars 96,[4] Mars Exploration Rover,[5] Phobos,[6] Mars Science Laboratory and the Philae comet lander.[7][8] APS/APXS devices will be included on several upcoming missions including the Chandrayaan-2 lunar rover.[9]

Sources

Several forms of radiation are used in APXS. They include alpha particles, protons, and X-rays. Alpha particles, protons, and X-rays are emitted during the radioactive decay of unstable atoms. A common source of alpha particles is curium-244. It emits particles with an energy of 5.8 MeV. X-rays of 14 and 18 keV are emitted in the decay of plutonium-240. The Mars Exploration Rovers' Athena payload uses curium-244 with a source strength of approximately 30 millicuries (1.1 GBq).[10]

Alpha particles
Sojourner takes its APXS measurement of the Yogi Rock.

Some of the alpha particles of a defined energy are backscattered to the detector if they collide with an atomic nucleus. The physical laws for Rutherford backscattering in an angle close to 180° are conservation of energy and conservation of linear momentum. This makes it possible to calculate the mass of the nucleus hit by the alpha particle.

Light elements absorb more energy of the alpha particle, while alpha particles are reflected by heavy nuclei nearly with the same energy. The energy spectrum of the scattered alpha particle shows peaks from 25% up to nearly 100% of the initial alpha particles. This spectrum makes it possible to determine the composition of the sample, especially for the lighter elements. The low backscattering rate makes prolonged irradiation necessary, approximately 10 hours.

Protons

Some of the alpha particles are absorbed by the atomic nuclei. The [alpha,proton] process produces protons of a defined energy which are detected. Sodium, magnesium, silicon, aluminium and sulfur can be detected by this method. This method was only used in the Mars Pathfinder APXS. For the Mars Exploration Rovers the proton detector was replaced by a second alpha particle sensor. So it is also called alpha proton X-ray spectrometer.

X-ray

The alpha particles are also able to eject electrons from the inner shell (K- and L-shell) of an atom. These vacancies are filled by electrons from outer shells, which results in the emission of a characteristic X-ray. This process is termed particle-induced X-ray emission and is relatively easy to detect and has its best sensitivity and resolution for the heavier elements.

Specific instruments
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References
  1. Economou, T.E.; Turkevich, A.L.; Sowinski, K.P.; Patterson, J.H.; Franzgrote, E.J. (1970). "The Alpha-Scattering Technique of Chemical Analysis". Journal of Geophysical Research. 75 (32): 6514. Bibcode:1970JGR....75.6514E. doi:10.1029/JB075i032p06514.
  2. Patterson, J.H.; Franzgrote, E.J.; Turkevich, A.L.; Anderson, W.A.; Economou, T.E.; Griffin, H.E.; Grotch, S.L.; Sowinski, K.P. (1969). "Alpha-scattering experiment on Surveyor 7 - Comparison with Surveyors 5 and 6". Journal of Geophysical Research. 74 (25): 6120–48. Bibcode:1969JGR....74.6120P. doi:10.1029/JB074i025p06120.
  3. R. Rieder; H. Wänke; T. Economou; A. Turkevich (1997). "Determination of the chemical composition of Martian soil and rocks:The alpha proton X ray spectrometer". Journal of Geophysical Research. 102 (E2): 4027–4044. Bibcode:1997JGR...102.4027R. doi:10.1029/96JE03918.
  4. Rieder, R.; Wanke, H.; Economou, T. (1997). "An Alpha Proton X-Ray Spectrometer for Mars-96 and Mars Pathfinder". American Astronomical Society. 28: 1062. Bibcode:1996DPS....28.0221R.
  5. R. Rieder; R. Gellert; J. Brückner; G. Klingelhöfer; G. Dreibus; A. Yen; S. W. Squyres (2003). "The new Athena alpha particle X-ray spectrometer for the Mars Exploration Rovers". Journal of Geophysical Research. 108 (E12): 8066. Bibcode:2003JGRE..108.8066R. doi:10.1029/2003JE002150.
  6. Hovestadt, D.; Andreichikov, B.; Bruckner, J.; Economou, T.; Klecker, B.; Kunneth, E.; Laeverenz, P.; Mukhin, L.; et al. (1988). "In-Situ Measurement of the Surface Composition of the Mars Moon Phobos: The Alpha-X Experiment on the Phobos Mission". Abstracts of the Lunar and Planetary Science Conference. 19: 511. Bibcode:1988LPI....19..511H.
  7. http://www.uni-mainz.de/, Johannes Gutenberg Universität Mainz, Alpha particle x-ray spectrometer developed in Mainz to be used on comet Churyumov–Gerasimenko, 10 April 2014
  8. "Alpha Proton X-ray Spectrometer (APXS) - Mission Name: Philae". NASA. 26 August 2014.
  9. "Payloads for Chandrayaan-2 Mission Finalised". isro.gov.in. Indian Space Research Organisation. 30 August 2010. Archived from the original on 15 October 2012. Retrieved 7 August 2012.
  10. unknown. "Alpha Particle X-Ray Spectrometer (APXS) (2 pages)" (PDF).
  11. JPL QuickLook - Phobos 1, 2
  12. SMALL AUTONOMOUS STATIONS - Mars 96
  13. Mars Pathfinder Instrument Descriptions - NASA
  14. ATHENA - Cornell University
  15. "Mars Exploration Rovers: Spacecraft: Surface Operations: Instruments: Alpha Particle X-Ray Spectrometer (APXS)". NASA JPL.
  16. NASA - Alpha Particle X-ray Spectrometer (APXS)
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